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Diffraction User Center

High-Temperature Synchrotron X-Ray Diffractometer at the National Synchrotron Light Source

 
 

This high-flux beamline instrument is designed to permit the measurement of precise lattice parameters.

Features:

  • Six-circle Huber diffractometer with split chi-ring; crystal analyzers (Si, Ge, LiF, graphite); CAMAC multichannel analyzer; pinholes > 10 mm diam; scintillation and proportional counters
  • Focusing incident beam silicon monochromator
  • Tunable wavelengths from 0.5 to 2.5 Å
  • Buehler HDK 2.3 furnace with Pt, W, Ta, or Mo strip heaters (RT to 1600°C , or 2200°C+ in vacuum) Controlled environment (O2, Ar, N2, H2, ambient, etc.), 1 atm
  • Rotating capillary mount and optional furnace

Applications:

  • Oxidation/reduction kinetics
  • Phase equilibria studies
  • Order/disorder transformations
  • Single-crystal diffraction
  • Rietveld analysis

 

 


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