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Diffraction User Center

High-Temperature X-Ray Powder Diffractometer

 
 

This instrument combines divergent optics with a high-temperature stage and atmospheric control.

Features:

  • Scintag PAD X vertical θ/θ goniometer
  • Cu, Mo, Cr, Co, Ag, and Fe x-ray targets
  • Buehler HDK 2.3 furnace with Pt, W, Ta, or
  • Mo strip heaters (RT to 1600°C , or 2200°C+ in vacuum)
  • Controlled environment (O2, Ar, N2, H2, ambient, etc.), 1 atm , pO2 sensing
  • Peltier Si(Li) energy-dispersive detector
  • Position-sensitive detector (rapid data acquisition)

Applications:

  • In situ
  • process simulation
  • Lattice thermal expansion coefficients
  • Oxidation/reduction kinetics
  • Phase equilibria studies
  • Order/disorder transformations
  • Rietveld analysis

 

 


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