David T. Hoelzer
Fusion Materials Program
Oak Ridge National Laboratory
Post Office Box 2008
Oak Ridge, TN 37831-6136
Tel: 865-574-5096
hoelzerd@ornl.gov
 

RESEARCH INTEREST Structure/property relationships of metals, alloys, intermetallics, and advanced ceramics; transmission electron microscopy (TEM); application of TEM and crystallography to crystal structure analysis and phase transformations; deformation behavior of alloys and intermetallics, development of high temperature structural materials, and mechanical alloying processing.

EDUCATION

  • Ph.D. in Materials Science and Engineering, University of Florida, Gainesville, December 1996.
    • Dissertation - "Phase Transformations in the Central Portion of the Nb-Ti-Al Ternary System."
  • M.S. in Materials Science and Engineering, University of Florida, Gainesville, December 1991.
    • Thesis - "The Effect of Copper and Nickel on the Neutron Irradiation Damage in Iron Alloys."
  • B.S. in Materials Science and Engineering, University of Florida, Gainesville, August 1985.
    • Senior Research - Investigated the ductile crack initiation process for an A-543 pressure vessel steel by correlating the stretch zone width with the crack tip opening displacement of the crack.

EMPLOYMENT HISTORY

Research Staff Member — Metals & Ceramics Division, Oak Ridge National Laboratory, Oak Ridge, TN. May 2000 to present. Current research projects:

Principle investigator of LDRD project investigating a new phenomena involving the formation of stable oxygen-rich nanoclusters in a ferritic alloy that was mechanically alloyed with yttria resulting in a dramatic improvement in high temperature strength over existing iron-based alloys.

Co-principle investigator on I-NERI project collaborating with scientists from CEA-Saclay in France investigating the deformation and fracture behavior of advanced nano-composited steels for high temperature structural applications in nuclear energy reactors.

Investigating solute interactions between Ti and interstitial O, C, and N impurities by studying the dynamic strain aging deformation behavior of V-4Cr-4Ti and vanadium.

Investigating the precipitation behavior and developing a process for redistributing interstitial O, C, and N solutes by controlled precipitation to improve properties of V-4Cr-4Ti, such as the low temperature fracture toughness and radiation hardening and the high temperature creep strength.

Post-Doctoral Research Fellowship — Metals & Ceramics Division, Oak Ridge National Laboratory, Oak Ridge, TN. September 1998 to May 2000.

Conducted research on various projects based on structure/property/processing relationships relevant to the Fusion Energy Program.

TEM Technical Specialist and Adjunct Instructor - New York State College of Ceramics at Alfred University (NYSCC), Alfred, NY. August 1992 to August 1998.

Instructor of graduate level TEM course which included lecture and laboratory sessions covering microscope components and operation, electron diffraction, amplitude and phase contrast image formation, image/diffraction interpretation, and specimen preparation for materials science applications.

Worked with faculty, students, and industrial clients in the area of analytical TEM characterization. Responsible for generating and interpreting data from imaging, diffraction, and x-ray energy dispersive spectroscopy (XEDS) techniques appropriate to the needs of specific projects. Also, instructed and performed suitable specimen preparation methodologies.

Manager of the TEM facility: JEOL 2000FX Analytical/Scanning Transmission Electron Microscope, PGT XEDS analyzer, Gatan DuoMill Ion-Mill, Edwards carbon evaporator, other specimen preparation equipment, and photographic darkroom facilities.

Graduate Research Assistant - Department of Materials Science and Engineering, University of Florida, Gainesville, FL. September 1985 to August 1987 and May 1988 to December 1991.

TEM Microscopist (part-time) - Major Analytical Instrumentation Center (MAIC), University of Florida, Gainesville, FL. August 1987 and May 1988.

MEMBERSHIP IN PROFESSIONAL ASSOCIATIONS

Materials Research Society (MRS)
Microscopy Society of America (MSA)
ASM International
Executive Committee Member; Oak Ridge Chapter, 1999 to present.
Executive Committee Member; S.W. New York Chapter, 1996-1998.
Sigma Xi
Air Force Association (AFA).

RESEARCH PUBLICATIONS

  • Stability of Ti-, Y-, and O-Enriched Particles in a MA/ODS Ferritic Alloy, M.K. Miller, D.T. Hoelzer, S.S. Babu, E.A. Kenik, and K. F. Russell, to be presented at the 49th International Field Emission Symposium, will be published in the J. de Physique, (2002).
  • Atom Probe Tomography of Nanoscale Particles in ODS Ferritic Alloys, M.K. Miller, E.A. Kenik, K.F. Russell, D.T. Hoelzer, and P.J. Maziasz, accepted in 2001 for publication in Mater. Sci. and Eng. A.
  • Investigating Solute Interactions in V-4Cr-4Ti Based on Tensile Deformation Behavior of Vanadium, D.T. Hoelzer and A.F. Rowcliffe, presented at ICFRM-10 in Baden-Baden in 2001, will be published in J. Nuclear Materials.
  • Effect of Periodic Temperature Variations on the Microstructure of Neutron Irradiated Metals, S.J. Zinkle, N. Hasimoto, D.T. Hoelzer, A.L. Qualls, T. Muroga, and B.N. Singh, presented at ICFRM-10 in Baden-Baden in 2001, will be published in J. Nuclear Materials.
  • Templated Growth of a Complex Nitride Island Dispersion Through an Internal Nitridation Reaction, M.P. Brady, D.T. Hoelzer, E.A. Payzant, P.F. Tortorelli, J.A. Horton, I.M. Anderson, L.R. Walker, and S.K. Wrobel, J. Mater. Res., 16:10, (2001), p. 2784.
  • A Microstructural Study of Oxide Scale Formation on ODS Fe-13Cr Steel, D.T. Hoelzer, B.A. Pint, and I.G. Wright, J. Nuclear Materials, 283-287, (2000), p. 1306.
  • Solute Interactions in Pure Vanadium and V-4Cr-4Ti Alloy, D.T. Hoelzer, M.K. West, S.J. Zinkle, and A.F. Rowcliffe, J. Nuclear Materials, 283-287, (2000), p. 616.
  • Effect of Strain Rate on the Tensile Properties of Unirradiated and Irradiated V-4Cr-4Ti, A.F. Rowcliffe, S.J. Zinkle, and D.T. Hoelzer, J. Nuclear Materials, 283-287, (2000), p. 508.
  • Development of an Oxide Dispersion Strengthened, Reduced-Activation Steel for Fusion Energy, G.R. Romanoski, L.L. Snead, R.L. Klueh, and D.T. Hoelzer, J. Nuclear Materials, 283-287, (2000), p. 642.
  • Impurity Effects on Gas Tungsten Arc Welds in V-Cr-Ti Alloys, M.L. Grossbeck, J.F. King, and D.T. Hoelzer, J. Nuclear Materials, 283-287, (2000), p. 1356.
  • Microstructures in Ti-Al Intermetallic Compounds Irradiated at 673K in HFIR, Y. Miwa, T. Sawai, K. Fukai, D.T. Hoelzer, and A. Hishinuma, J. Nuclear Materials, 283-287, (2000), p. 273.
  • An Electron Microscopy Study of the Formation of Hydroxyapatite Through Sol-Gel Processing, A. Jillavenkatesa, D.T. Hoelzer, and R.A. Condrate, J. Materials Science, 34, (1999), p. 4821.
  • Grain Boundaries and Growth Kinetics of Polycrystalline Ferrimagnetic Oxides with Chemical Additives, Y.S. Cho, D.T. Hoelzer, V.L. Burdick, and V.R.W. Amarakoon, J. Applied Physics, 85:8, (1999), p. 1.
  • Cordierite-Based Dielectric Thick Films on an Oxidized Copper Layer: Microstructural Evidence of Copper Diffusion, Y.S. Cho, D.T. Hoelzer, W. Schulze, and V.R.W. Amarakoon, J. American Ceramic Society,
    82:7, (1999), p. 1949.
  • Crystallization and Microstructural Evolution of Cordierite-Based Thick Film Dielectrics, Y.S. Cho, D.T. Hoelzer, W.A. Schulze, and V.R.W. Amarakoon, Acta Mater., 46:18, (1998), p. 6421.
  • Interfacial Characterization of Plasma-Sprayed Calcium Phosphate Coatings on Ti-6Al-4V, E. Park, R.A. Condrate, Sr., D.T. Hoelzer, and G.S. Fischman, J. Materials Science: Materials in Medicine,
    9:11, (1998), p. 643.
  • The Effect of Aluminum on the Formation of Orthorhombic Plates in the Nb-Ti-Al Ternary System, D.T. Hoelzer and F. Ebrahimi, High-Temperature Ordered Intermetallic Alloys VII, MRS Symposium Proceeding, Materials Research Society, 460, (1997), p. 97.
  • Analysis of the Interface Between Plasma-Sprayed Hydroxyapatite Coating and Ti, E. Park, D.T. Hoelzer, and R.A. Condrate, Thin Films, MRS Symposium Proceeding, Materials Research Society, 458, (1997), 
    p. 409.
  • Interactions at Metal/InP Interfaces Formed at 300K and 77K, J. Palmer, W. Anderson, D.T. Hoelzer, and H. Hardtdegen, Compound Semiconductor Electronics and Photonics, MRS Symposium Proceeding, Materials Research Society, 421, (1996), p. 257.
  • Grain-Oriented Ferroelectric Bismuth Titanate Thin Films Prepared from Acetate Precursor, Y. Lu, D.T. Hoelzer, W. Schulze, B. Tuttle, and B.G. Potter, Mat. Sci. Eng., B39, (1996), p. 41.
  • Cross-Sectional TEM of Pd/InP and Au/InP Interfaces Formed at Substrate Temperatures Near 300K and 77K, J.W. Palmer, W.A. Anderson, D.T. Hoelzer, and M. Thomas, J. Electronic Materials, 25, (1996), p. 1645.
  • Modification of Microstructure for Improved Oxidation Resistance in Gamma-Based Ti-Al-X Alloys, M.P. Brady, J.L. Smialek, E.D. Verink, Jr., D.T. Hoelzer, and R. Stone, Materials and Manufacturing Processes, 11:4, (1996), p. 635.
  • Examination of Y2Cu2O5 Additions on Microstructural Development in YBa2Cu3O7-d Superconductors, J.G. Fagan, K.D. Vuong, D.T. Hoelzer, X.W. Wang, C.Q. Shen, V.R. Amarakoon, and R.L. Snyder, Applied Superconductivity, 3:1-3, (1995), p. 91.
  • Effect of Copper and Nickel on the Neutron Irradiation Damage in Iron Alloys, D.T. Hoelzer and F. Ebrahimi, Microstructure in Irradiated Materials, MRS Symposium Proceeding, Materials Research Society, 373, (1995), p. 57.
  • High Resolution Microscopy of Pd/InP Interfaces, J.W. Palmer, W.A. Anderson, and D.T. Hoelzer, Evolution of Thin Film and Surface Structure and Morphology, MRS Symposium Proceeding, Materials Research Society, 355, (1995), p. 477.
  • Grain Growth Behavior of Bismuth Titanate Thin Film on Metallic Silicon Substrates, Y. Lu and D.T. Hoelzer, Evolution of Thin Film and Surface Structure and Morphology, MRS Symposium Proceeding, Materials Research Society, 355, (1995), p. 607.
  • Photosensitivity in a Silica-Based Sol-Gel Glass, D.M. Korwin, D.T. Hoelzer, and L.D. Pye, Symposium Proceeding on Preparation of Materials Via Soft Chemistry, 97th Annual Meeting, (1995).
  • Ferroelectric Thin Film Bismuth Titanate Prepared from Acetate Precurser, Y. Lu, D.T. Hoelzer, W.A. Schulze, B. Tuttle, and B.G. Potter, Penn. State Conference on Ferroelectrics, Aug. 1994.
  • Fracture Toughness of  + x Microstructures in the Nb-Ti-Al System, F. Ebrahimi, D.T. Hoelzer, and J.R. Castillo-Gomez, Materials Science and Engineering, A171, (1993), p. 35.
  • The Effect of Rapid Solidification on the Oxidation Behavior of a Nb-Ti-Al Alloy, M.P. Brady, R.K. Stone, D.T. Hoelzer, S.P. Elder-Randall, and E.D. Verink, Jr., in "Processing and Fabrication of Advanced Materials for High Temperature Applications," Eds: T.S. Srivatsan and V.A. Ravi, TMS, (1992), p. 239-248.
  • An Investigation of Phase Stability in the Ternary Niobium-Titanium-Aluminum System, D.T. Hoelzer and F. Ebrahimi, in "High Temperature Niobium Alloys," TMS, Warrendale, PA (1991), p. 105.
  • The Effect of Copper and Nickel on the Neutron Irradiation Damage in Iron Alloys, D.T. Hoelzer, MS Thesis, Univ. of Florida, (1991).
  • Phase Stability of Sigma + Beta Microstructures in the Ternary Nb-Ti-Al System, D.T. Hoelzer and F. Ebrahimi, Material Research Society Symposium Proceeding, Materials Research Society, Vol. 194, (1990), p. 393.
  • Development of a Mechanistic Understanding of Radiation Embrittlement in Reactor Pressure Vessel Steels, F. Ebrahimi, D.T. Hoelzer, D. Venables, and V. Krishnamoorthy, Final Report NUREG/CR-5063 MEA-2268, (1988).
  • Microstructural Characterization of Irradiated Fe-Cu-Ni-P Model Steels, M.K. Miller, D.T. Hoelzer, F. Ebrahimi, J.R. Hawthorne, and M.G. Burke, in "Environmental Degradation of Materials in Nuclear Power Systems-Water Reactors," TMS/AIME, Warrendale, PA (1988), p. 133.
  • On the Effect of Cu on -Carbide Nucleation, F. Ebrahimi, B. Hoover, and D.T. Hoelzer, Scripta Metallurgica, Vol. 22, (1988), p. 219.
  • Characterization of Irradiated Model Pressure Vessel Steels, M.K. Miller, D.T. Hoelzer, F. Ebrahimi, J.R. Hawthorne, and M.G. Burke, Journal De Physique, Colloque 6, (1987), p. 423.
  • A Study of the Correlation Between Crack Tip Opening Displacement (CTOD) and Stretch Zone Width (SZW), D.T. Hoelzer, J.A. Ali, and F. Ebrahimi, Scripta Metallurgica, Vol. 20, (1986), p. 1575.

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