Group scientists and collaborators have pioneered many new x-ray techniques with a special emphasis on anomalous (resonant) x-ray diffraction. Advanced x-ray characterization supported by the group includes:

  • Anomalous diffuse x-ray scattering for characterization of short-range correlations in alloys and bond distances to ± 0.001;

  • Truncation rod scattering for measurement of surface and interface roughness, atomic structure and chemistry;

  • Microfluorescence analysis/tomography (<1 mm2; <10 mm3) for the study of sample chemistry at part-per-billion (PPB) sensitivity;

  • Microdiffraction (<1 mm2) for the study of inhomogeneous phase, texture and strain over small volumes;

  • Anomalous powder diffraction for the study of site-occupation parameters;

  • Resonant magnetic scattering for the measurement of magnetic transitions.

  • Texture and residual stress in thin films.



Samples studied include:

  • Fe-Ni-Cr and other intermetallic alloys

  • Nonferrous alloys including nickel-based superalloys, aluminum- and vanadium-based alloys

  • High temperature superconductors

  • Structural ceramics

  • Advanced electronic materials

  • Composites

  • Graphite and diamond materials

  • Phase transformations in magnetic and non-magnetic materials

  • Thin films and buried interfaces

  • Amorphous and rapidly solidified materials.

  • Radiation effects in a wide-range of materials including segregation, stress, corrosion, and diffusion.

 

 




The X-ray Research and Applications Group has access to unique x-ray characterization facilities such as beamline X14A at the NSLS. This beamline is highly optimized for anomalous (resonant) x-ray diffraction.



Diffuse x-ray scattering map of an Fe-Ni Invar alloy is sensitive to local chemical order and chemically specific bond distances.