|


Group scientists
and collaborators have pioneered many new x-ray techniques with a special
emphasis on anomalous (resonant) x-ray diffraction. Advanced x-ray characterization
supported by the group includes:

- Anomalous
diffuse x-ray scattering for characterization of short-range correlations
in alloys and bond distances to ± 0.001;

- Truncation
rod scattering for measurement of surface and interface roughness, atomic
structure and chemistry;

- Microfluorescence
analysis/tomography (<1 mm2; <10 mm3) for the study of sample chemistry
at part-per-billion (PPB) sensitivity;

- Microdiffraction
(<1 mm2) for the study of inhomogeneous phase, texture and strain over
small volumes;

- Anomalous
powder diffraction for the study of site-occupation parameters;

- Resonant
magnetic scattering for the measurement of magnetic transitions.

- Texture
and residual stress in thin films.

Samples studied include:

- Fe-Ni-Cr
and other intermetallic alloys

- Nonferrous
alloys including nickel-based superalloys, aluminum- and vanadium-based
alloys

- High temperature
superconductors

- Structural
ceramics

- Advanced
electronic materials

- Composites

- Graphite
and diamond materials

- Phase
transformations in magnetic and non-magnetic materials

- Thin films
and buried interfaces

- Amorphous
and rapidly solidified materials.

- Radiation
effects in a wide-range of materials including segregation, stress,
corrosion, and diffusion.
|
The X-ray
Research and Applications Group has access to unique x-ray characterization
facilities such as beamline X14A at the NSLS. This beamline is highly
optimized for anomalous (resonant) x-ray diffraction.
Diffuse x-ray
scattering map of an Fe-Ni Invar alloy is sensitive to local chemical
order and chemically specific bond distances.
|